32005-36-0, Name is Bis(dibenzylideneacetone)palladium, belongs to catalyst-palladium compound, is a common compound. Formula: C34H28O2PdIn an article, once mentioned the new application about 32005-36-0.
The invention discloses a high-purity (dibenzylidene acetone) two palladium (0) of the preparation method, the method comprises: a, under the nitrogen atmosphere, the ligand dibenzylidene acetone, two palladium chloride and anhydrous sodium acetate into a mixing state in anhydrous ethanol heating reaction, obtained after filtering the solid double-(dibenzylidene acetone) palladium (0); b, under the nitrogen atmosphere, obtained in the step a solid double-(dibenzylidene acetone) palladium (0) into a mixing state of acetone in the reaction, washing of objects after being filtered, washed and removing of drying, to obtain three (dibenzylidene acetone) two palladium (0). The invention uses absolute ethanol, dibenzylidene acetone, two palladium chloride and anhydrous sodium acetate first preparing double-(dibenzylidene acetone) palladium (0), then the acetone solution processing to obtain three (dibenzylidene acetone) two palladium (0), the prepared three (dibenzylidene acetone) two palladium (0) of relatively high purity. (by machine translation)
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Reference：
Chapter 1 An introduction to palladium catalysis,
Palladium/carbon catalyst regeneration and mechanical application method