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Synthesis of 1-substituted 1-siloxy-3-aryloxybuta-1,3-dienes is achieved starting with readily available methyl ketones by a reaction sequence involving a palladium-catalyzed addition of the ketone to a 3,5-xylyl triisopropylsilylethynyl ether followed by isomerizations. This synthetic method is applicable to various methyl ketones. Cycloaddition of the resulting dienes with electron-deficient alkenes and alkynes gives 6-membered carbo- and heterocycles.
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Reference：
Chapter 1 An introduction to palladium catalysis,
Palladium/carbon catalyst regeneration and mechanical application method